The utility model discloses an electrode modification reaction device, which comprises a base and an upper cover; an electrode placement position is arranged on the base, and a plurality of elastic components of clamping electrodes are arranged in the electrode placement position; the outer cover can be detachably connected to the base, and a sealing member is arranged between the outer cover and the base to form a closed reaction space for the inner cavity of the outer cover; and the side wall of the base is provided with an entry connected with the reaction space. The top of the hood is provided with an air outlet. In the experiment, the electrodes are inserted into the electrodes and clamped by elastic components to keep the electrodes stable during the modification process. After clamping and positioning, liquid is added. Then the outer cover is detachably connected to the base, and inert gas is filled into the bottom intake port to discharge the air from the top outlet in the reaction space, and then the air intake and outlet are closed. In order to keep the electrode in a clean and windless reaction environment during the modification process, the surface of the electrode can be avoided from being polluted and the phenomenon of liquid dispersion caused by wind blowing can be avoided.
【技术实现步骤摘要】
电极修饰反应装置
本技术属于电极修饰实验设备领域,尤其涉及一种电极修饰反应装置。
技术介绍
电化学电极在研究及实验过程中需要在其表面进行涂覆修饰,通常的修饰过程中,需要将电极倒置,在电极表面滴加液体,由其自然挥发干燥,长时间的干燥过程中需要避免灰尘等颗粒物污染电极表面,一般在其上放置一个罩子。但在整个过程中,没有一个统一完整的装置可以进行使用,且对于易氧化的修饰反应,通气体变得更加复杂。而目前的装置均不能保证电极竖直设置,使电极表面的溶液难以均布,修饰效果较差,另一方面目前实验过程中电极修饰是否完成均通过经验判断,初次实验者难以把控。
技术实现思路
本技术的目的在于提供一种能够防止电极表面被污染且修饰效果可靠的电极修饰反应装置。本技术提供的这种电极修饰反应装置,它包括底座和上罩;底座上设有电极放置位,电极放置位内设多对夹紧电极的弹性构件;外罩可拆卸连接于底座上,外罩与底座之间设有密封构件使外罩的内腔形成可密闭的反应空间;底座的侧壁设有与反应空间连通的进气口,外罩的顶部设有出气口。在一个具体实施方式中,为了保证电极修饰时处于竖直状态,使所述底座为圆柱型座体,所述电极放置位为 ...
【技术保护点】
1.一种电极修饰反应装置,其特征在:它包括底座和上罩;底座上设有电极放置位,电极放置位内设多对夹紧电极的弹性构件;外罩可拆卸连接于底座上,外罩与底座之间设有密封构件使外罩的内腔形成可密闭的反应空间;底座的侧壁设有与反应空间连通的进气口,外罩的顶部设有出气口。
【技术特征摘要】
1.一种电极修饰反应装置,其特征在:它包括底座和上罩;底座上设有电极放置位,电极放置位内设多对夹紧电极的弹性构件;外罩可拆卸连接于底座上,外罩与底座之间设有密封构件使外罩的内腔形成可密闭的反应空间;底座的侧壁设有与反应空间连通的进气口,外罩的顶部设有出气口。2.根据权利要求1所述的电极修饰反应装置,其特征在于:所述底座为圆柱型座体,所述电极放置位为设置于底座上的竖直盲孔,每对所述弹性构件均为关于竖直盲孔轴向中心面对称设置的两个金属弹片。3.根据权利要求2所述的电极修饰反应装置,其特征在于:所述底座内设电源,底座外设循环...
【专利技术属性】
技术研发人员:刘亮亮,肖爱平,梅时勇,冷鹃,杨喜爱,廖丽萍,
申请(专利权)人:中国农业科学院麻类研究所,
类型:新型
国别省市:湖南,43
还没有人留言评论。发表了对其他浏览者有用的留言会获得科技券。