A method of microwave method of one-step synthesis of PdPt/ graphene nano electrocatalysts, graphene oxide dispersed in aqueous solution of quaternary ammonium surfactant, adding soluble PdII salt and PtII salt solution, fully mixed, adjusting the pH of mixed solution, adding reducing agent, mixing reaction in microwave the radiation at the same time, the reduction of palladium and platinum metal ions and graphene oxide, the reaction product of cooling, washing and drying to obtain the nano graphene electrocatalysts PdPt/. The invention has the advantages of energy saving, environmental protection, fast and simple process, etc. the obtained PdPt/ graphene electrocatalyst has good electrocatalytic performance for the electrochemical oxidation of methanol.
【技术实现步骤摘要】
【技术保护点】
１．一种微波法一步合成ＰｄＰｔ／石墨烯纳米电催化剂的方法，其特征在于将氧化石墨烯超声分散在季铵盐型表面活性剂的水溶液中，加入可溶性ＰｄＩＩ盐和ＰｔＩＩ盐溶液，充分混合均匀，调节混合溶液的ｐＨ值，并加入还原剂，混合均匀后在微波的辐射下反应，同时还原钯、铂金属离子和氧化石墨烯，反应产物冷却、洗涤、干燥即可得到ＰｄＰｔ／石墨烯纳米电催化剂。
【技术特征摘要】
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